Tracers / [11C]acetoacetate

[11C]acetoacetate

Also written as [11C]Acetoacetate; [C-11]Acetoacetate
Radionuclide
C-11 t½ 20.36 min
Modality
PET
Production route
Stage
Syntheses indexed
3

What it is

Compound class
carboxylic acid (short-chain ketone body, acetoacetate)
Target / mechanism
Clinical application
Theranostic pair

Regulatory status

FDA
EMA (centralised)
Other approvals
Brand names

Clinical use

Typical injected activity
Uptake time

Reported in the literature. Not a dosing recommendation.

Published syntheses

ModuleCassettePurificationYield %RCP %Precursor / supplierSource
TRACERlab FX2 C
GE HealthCare
custom manifoldHPLC4.67 ± 1.36%
yes
97.1 ± 1.3%lithium enolate of acetone (from isopropenyl acetate and MeLi)
Sigma-Aldrich
41452397
2025 EJNMMI Radiopharm Chem
a GE TRACERlab FX2 C module — The decay-corrected RCY was 4.67 ± 1.36% after an average synthesis time of 15 min
GE HealthCare
custom manifoldSPE16.1 ± 1.1%
no
97 ± 2%chloroacetone (17-Cl)37608567
2024 J Labelled Comp Radiopharm
Following the standard automated [11C]carbonylation protocol, the loop mixture was quenched with 0.1M NaOH — corresponding to 16.1 ± 1.1% non-decay corrected RCY
AllinOne (AiO)
Trasis
SPE35%
yes
95%isopropenylacetate (IPA)
Sigma-Aldrich
28806598
2017 Appl Radiat Isot
TRASIS AllInOne (AIO) is a commonly used radiochemistry module for clinical GMP-grade radiopharmaceutical production — 1-[11C]acetoacetate was synthesized with high radiochemical purity (95%) and specific activity (~ 66.6 GBq/µmol, n = 30) with 35% radiochemical yield, decay corrected to end of synthesis.

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Quality control Preliminary — inferred from compound class

Ph. Eur. monograph
USP monograph
AppearancepHRCP HPLCRCP TLCHPLC UVRadionuclidic (HPGe)Half-lifeActivityEndotoxins (LAL)SterilityFilter integrityMolar activity
How this set was arrived at. base set per Ph. Eur. general monograph 0125 (rule); receptor ligand with a saturable target -> molar activity (rule); organic-phase radiosynthesis assumed from isotope/compound class, no synthesis data confirming it -> GC residual solvents (preliminary)

Tests listed by reference only. Monograph texts are copyrighted and are not reproduced here. How these are derived

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Notes

Added from reverse module search (stage 6); 2 article(s) with C-11.