Tracers / [11C]6-bromopurine

[11C]6-bromopurine

Also written as [11C]6-bromopurine; [C-11]6-bromopurine
Radionuclide
C-11 t½ 20.36 min
Modality
PET
Production route
Stage
preclinical (non-clinical toxicity study and human dosimetry estimates, prepared to advance to clinical use)
Syntheses indexed
2

What it is

Compound class
6-bromo-7-methylpurine derivative (small-molecule purine analogue)
Target / mechanism
Measures multidrug resistance-associated protein 1 (MRP1) transport activity PMID 38683266
Clinical application
Theranostic pair

Regulatory status

FDA
EMA (centralised)
Other approvals
Brand names

Clinical use

Typical injected activity
Uptake time

Reported in the literature. Not a dosing recommendation.

Published syntheses

ModuleCassettePurificationYield %RCP %Precursor / supplierSource
TRACERlab FX C Pro
GE HealthCare
16.8 ± 1.7 %
yes
>98 %6-bromopurine27090254
2016 EJNMMI Res
in a Tracerlab FX C Pro synthesis module with slight modifications compared to the literature — [11C]7m6BP was obtained in a radiochemical yield of 16.8 ± 1.7 % (n = 12) (based on [11C]methyl triflate, decay-corrected)
TRACERlab FX2 C
GE HealthCare
fixed tubingHPLC+SPE20.5 ± 5.2%
yes
>99%6-bromo-7H-purine
Mihulka, s.r.o., Opava-Jaktar, Czech Republic
38683266
2024 EJNMMI Radiopharm Chem
The automated radiosynthesis was performed in a TRACERlab™ FX2 C synthesis module (GE Healthcare, Uppsala, Sweden). — decay-corrected radiochemical yield of 20.5 ± 5.2%, based on starting [11C]methyl iodide

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Quality control Preliminary — inferred from compound class

Ph. Eur. monograph
USP monograph
AppearancepHRCP HPLCRCP TLCHPLC UVRadionuclidic (HPGe)Half-lifeActivityEndotoxins (LAL)SterilityFilter integrity
How this set was arrived at. base set per Ph. Eur. general monograph 0125 (rule); organic-phase radiosynthesis assumed from isotope/compound class, no synthesis data confirming it -> GC residual solvents (preliminary)

Tests listed by reference only. Monograph texts are copyrighted and are not reproduced here. How these are derived

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Notes

Added from reverse module search (stage 6); 2 article(s) with C-11. Compound class inferred from precursor name (not stated outright) -- PMID 38683266: '6-Bromo-7H-purine was synthesised with a purity of 99.2% (HPLC) by Mihulka, s.r.o.'. Stage set/updated at stage 23 from PMID 38683266: 'Advancing 6-bromo-7-[11C]methylpurine to clinical use: improved regioselective radiosynthesis, non-clinical toxicity data and human dosimetry estimates.'.