Tracers / [18F]fluoroethylcholine

[18F]fluoroethylcholine

Also written as [18F]fluoroethylcholine; [F-18]fluoroethylcholine; Fluoroethylcholine
Radionuclide
F-18 t½ 109.77 min
Modality
PET
Production route
Stage
Syntheses indexed
11

What it is

Compound class
Target / mechanism
Clinical application
Theranostic pair

Regulatory status

FDA
EMA (centralised)
Other approvals
Brand names

Clinical use

Typical injected activity
Uptake time

Reported in the literature. Not a dosing recommendation.

Published syntheses

ModuleCassettePurificationYield %RCP %Precursor / supplierSource
TRACERlab FX FN
GE HealthCare
custom manifoldSPE5%
no
dibromomethane
Sigma-Aldrich
21769163
2011 J Labelled Comp Radiopharm
The TracerLab FXFN was configured as shown in Figure 11 — Typical non-decay corrected yields of [18F]fluoromethylcholine using this optimized production method were 5%, (n = 7).
SPE8 ± 3%97.3 ± 2.6%dimethylaminoethanol precursor33153893
2021 Appl Radiat Isot
We have used FX2C and FX2N Tracerlab modules for the synthesis of the [11C]methionine, [18F]choline and [18F]fluorodopa via nucleophilic pathway in FX2C/N module. — [18F]fluoromethylcholine was prepared with high radiochemical purity of 97.3 ± 2.6% with yield of 8 ± 3%.
SPE36%
no
ethyleneglycolditosylate19520298
2009 Nucl Med Biol
We used a Modular Lab system to automatically perform the two-step/one-pot synthesis. — The optimized procedure resulted in a non decay corrected yield of 36%
SPE15-25%
no
more than 99%N,N-dimethylaminoethanol18312837
2008 Nucl Med Biol
Fully automated [18F]fluorocholine synthesis in the TracerLab MX FDG Coincidence synthesizer. — the [18F]fluorocholine was obtained in 15-25% radiochemical yields (decay not corrected)
SPE17.8 ± 2.5 %>99 %Dibromomethane (DBM)40147115
2025 Appl Radiat Isot
synthesis, purification and formulation of [18F]FCH on the GE FASTlab II utilizing a single-use cassette was reported. — the radiochemical yield of [18F]FCH was 17.8 ± 2.5 %
SPE18.8 ± 2.1%>90%dibromomethane28734194
2017 Appl Radiat Isot
[18F]FCH was synthesized using a modified TRACERlab FxFN module. — the RCY of [18F]FCH was 18.8 ± 2.1% (EOB, n = 27)
SPE4-6%>99.7%21115355
2011 Appl Radiat Isot
modification of a GE TracerLab FX(FN) is reported which enables gas-phase production of [(18)F]fluoromethylcholine — in 4-6% RCY and >99.7% RCP
SPE37±5%>95%2-bromoethyl-4-nitrobenzenesulfonate (BENos)21315271
2011 Nucl Med Biol
The fully automated synthesis was performed using as well a Raytest SynChrom module (Raytest, Germany) or a Scintomics HotboxIII module (Scintomics, Germany). — 37±5% (Synchrom module)
SPE33±5%>95%2-bromoethyl-4-nitrobenzenesulfonate (BENos)21315271
2011 Nucl Med Biol
The fully automated synthesis was performed using as well a Raytest SynChrom module (Raytest, Germany) or a Scintomics HotboxIII module (Scintomics, Germany). — 33±5% (Hotbox III unit)
SPE47±5%
no
>99.9%2-bromoethyl triflate (BETfO)18819809
2008 Bioorg Med Chem
a modified, commercially available fully automated synthesis module — resulting in a total yield of 47+/-5% (not decay corrected) in only 40min
30±6%95-99%N,N-dimethylaminoethanol17346977
2007 Bioorg Med Chem
we established a reliable, fully automated synthesis for its production using a modified, commercially available module — resulting in a total radiochemical yield of 30+/-6% after a synthesis time of 50 min

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Quality control Preliminary — inferred from compound class

Ph. Eur. monograph
USP monograph
AppearancepHRCP HPLCRCP TLCHPLC cond.Residual solvents (GC)Radionuclidic (HPGe)Half-lifeActivityEndotoxins (LAL)SterilityFilter integrity
How this set was arrived at. base set per Ph. Eur. general monograph 0125 (rule); weak UV chromophore (sugar/simple ion/short-chain acid) -> conductometric detection (rule); organic solvent confirmed in synthesis data (PMID 21769163) -> GC residual solvents; conventional nucleophilic 18F-fluorination assumed from isotope/compound class, no synthesis data confirming K222 use -> Kryptofix test (preliminary)

Tests listed by reference only. Monograph texts are copyrighted and are not reproduced here. How these are derived

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Notes

Added from reverse module search (stage 6); 2 article(s) with F-18.