Tracers / [11C]UCB-J

[11C]UCB-J

Also written as [11C]UCB-J; [C-11]UCB-J; UCB-J
Radionuclide
C-11 t½ 20.36 min
Modality
PET
Production route
Stage
Syntheses indexed
4

What it is

Compound class
Pyrrolidinone SV2A ligand (trifluoroborate-derived, 11C-methylated small molecule)
Target / mechanism
Targets synaptic vesicle glycoprotein 2A (SV2A) to visualize synaptic density PMID 42154186
Clinical application
Imaging synaptic density in patients with epilepsy and other neurologic, neurodegenerative, or psychiatric conditions PMID 42154186
Theranostic pair

Regulatory status

FDA
EMA (centralised)
Other approvals
Brand names

Clinical use

Typical injected activity
Uptake time

Reported in the literature. Not a dosing recommendation.

Published syntheses

ModuleCassettePurificationYield %RCP %Precursor / supplierSource
Synthra RNplus
Synthra
custom manifoldHPLC+SPE11 ± 1% (nondecay corrected); 35 ± 4% (decay corrected)
no
100(R)-trifluoro(4-((2-oxo-4-(3,4,5-trifluorophenyl)pyrrolidin-1-yl)methyl)pyridin-1-ium-3-yl)borate (UCB-J precursor)
UCB, Belgium
32027052
2020 J Labelled Comp Radiopharm
Synthra RNPlus synthesizer — The nondecay corrected radiochemical yield was 11 ± 1% (n = 7) and if decay corrected 35 ± 4% (n = 7).
In-house / custom built
Siemens
72 ± 10%
yes
33238289
2021 Nature
our 11C-labeling protocol was independently performed by Siemens Molecular Imaging Biomarker Research in North Wales, PA with a robotic, remote-controlled radiosynthetic setup for the preparation of [11C]UCB-J — yielding 72 ± 10% RCY (dc) and 19 ± 2% RCY (ndc) (n = 4) of the radioligand
In-house / custom built
in-house
custom manifoldHPLC+SPE26.7 ± 5.6%
yes
99.3 ± 0.2%(R)-3-(difluoroboranyl)-4-((2-oxo-4-(3,4,5-trifluorophenyl)pyrrolidin-1-l)methyl)-pyridin-1-ium fluoride
PharmaSynth AS, Tartu, Estonia
42154186
2026 EJNMMI Radiopharm Chem
we present an in-house-built device for [11C]UCB-J production from [11C]CH3I and a suitably treated boronated precursor — 56 using new preparative HPLC method protocol 2 (RCY 26.7 ± 5.6%)
Synthra MeIplus
Synthra
HPLC+SPE21.1 ± 6.1%
yes
99.4 ± 0.2%(R)-3-(difluoroboranyl)-4-((2-oxo-4-(3,4,5-trifluorophenyl)pyrrolidin-1-l)methyl)-pyridin-1-ium fluoride
PharmaSynth AS, Tartu, Estonia
42154186
2026 EJNMMI Radiopharm Chem
[11C]CH3I production using the Synthra MeIplus Research device (Synthra GmbH, Hamburg, Germany) — 94 of these syntheses were performed using protocol 1 as preparative HPLC method (RCY 21.1 ± 6.1%)

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Quality control Preliminary — inferred from compound class

Ph. Eur. monograph
USP monograph
AppearancepHRCP HPLCRCP TLCHPLC UVRadionuclidic (HPGe)Half-lifeActivityEndotoxins (LAL)SterilityFilter integrity
How this set was arrived at. base set per Ph. Eur. general monograph 0125 (rule); organic-phase radiosynthesis assumed from isotope/compound class, no synthesis data confirming it -> GC residual solvents (preliminary)

Tests listed by reference only. Monograph texts are copyrighted and are not reproduced here. How these are derived

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Notes

Added from reverse module search (stage 6); 1 article(s) with C-11. Merged stage 17: +4 article(s) from c11-synvest1 (row was a mislabelled duplicate of [11C]UCB-J); combined count 5. Compound class inferred from precursor name (not stated outright) -- PMID 32027052: '(R)-trifluoro(4-((2-oxo-4-(3,4,5-trifluorophenyl)pyrrolidin-1-yl)methyl)pyridin-1-ium-3-yl)borate (UCB-J precursor)'.